Recently I am researching about H BOND ACTIVATION; SUPERCRITICAL CARBON-DIOXIDE; DIRECTING GROUP; O BOND; INTERNAL OXIDANT; POLYETHYLENE-GLYCOL; IONIC LIQUIDS; EFFICIENT SYNTHESIS; IRIDIUM COMPLEXES; ORGANIC-SYNTHESIS, Saw an article supported by the University Grant Commission (UGC), New Delhi, IndiaUniversity Grants Commission, India [F.25-1/2014-15(BSR)/F.7-227/2009]. Quality Control of 1-(4-Nitrophenyl)ethanone. Published in WILEY-V C H VERLAG GMBH in WEINHEIM ,Authors: Deshmukh, DS; Gangwar, N; Bhanage, BM. The CAS is 100-19-6. Through research, I have a further understanding and discovery of 1-(4-Nitrophenyl)ethanone
Herein, we report an atom-efficient, rapid, green, and sustainable approach to synthesize isoquinolines and isoquinolinones using a homogeneous recyclable ruthenium catalyst in PEG Media assisted by microwave energy. Dibenzoylhydrazine was used for C-H/N-N activation reactions for the first time in combination with ketazine as oxidizing directing groups for annulation reactions with internal alkynes. The developed protocol is environmentally benign due to significantly shortened times with an easy extraction method, higher atom economy, external oxidant and silver or antimony salt free conditions, applicability to a gram scale synthesis, use of biodegradable solvent and wide substrate scope with higher product yields. Moreover, it is worth noting that the established methodology allowed reuse of the catalytic system for up to five successive runs with minimal loss in activity.
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Reference:
Benzodioxan,
,1,4-Benzodioxane | C8H8O2 – PubChem