4442-54-0, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 2,3-Dihydro-1,4-benzodioxine-6-carboxylic acid, cas is 4442-54-0,the benzodioxans compound, it is a common compound, a new synthetic route is introduced below.
2,3-dihydrobenzo [b] [1,4] dioxine-6-carboxylic acid (5.0 g, 27.7 mmol, 1.0 equiv) was dissolved in DCM (100 mL). Thionyl chloride (15 mL) was added dropwise and the reaction mixture was stirred overnight at 70oC. The solvent was evaporated under reduced pressure to yield the pure product: 3.8 gr, 69 percent yield.
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 2,3-Dihydro-1,4-benzodioxine-6-carboxylic acid, 4442-54-0
Reference£º
Article; Yacovan, Avihai; Ozeri, Rachel; Kehat, Tzofit; Mirilashvili, Sima; Sherman, Daniel; Aizikovich, Alex; Shitrit, Alina; Ben-Zeev, Efrat; Schutz, Nili; Bohana-Kashtan, Osnat; Konson, Alexander; Behar, Vered; Becker, Oren M.; Bioorganic and Medicinal Chemistry Letters; vol. 22; 20; (2012); p. 6460 – 6468;,
Benzodioxan
1,4-Benzodioxane | C8H8O2 – PubChem