Zhang, S; Shi, XH; Li, JC; Hou, ZT; Song, ZH; Su, XF; Peng, D; Wang, F; Yu, YT; Zhao, GL in [Zhang, Shuo; Shi, Xinhua; Li, Jichao; Hou, Zitong; Song, Zihe; Su, Xiaofeng; Peng, Dan; Wang, Feng; Yu, Yitao] Qilu Univ Technol, Shandong Acad Sci, Adv Mat Inst, Shandong Prov Key Lab Special Silicone Containing, Jinan 250014, Shandong, Peoples R China; [Zhao, Guilong] Guangzhou Lixin Pharmaceut Inc, Dept Drug Discovery, Guangzhou 510535, Guangdong, Peoples R China published Nickel-Catalyzed Amidoalkylation Reaction of gamma-Hydroxy Lactams: An Access to 3-Substituted Isoindolinones in 2019, Cited 52. Category: benzodioxans. The Name is 1-(4-Nitrophenyl)ethanone. Through research, I have a further understanding and discovery of 100-19-6.
An efficient Ni(ClO4)(2)center dot 6H(2)O-promoted amidoalkylation re-action for the synthesis of 3-substituted isoindolinones involving various gamma-hydroxy lactams and nucleophiles has been successfully developed. The transformation proceeds with both carbon (ketones and arenes) and heteroatom (alcohols, thiols, and amines) nucleophiles and in both intermolecular and intramolecular manners. The prominent features of the present strategy are wide substrate scope, excellent group tolerability, and moderate to good yields (up to 96% yield). The present strategy is also characterized by remarkable superiority over the current synthetic methods. Furthermore, the reaction could be scaled up to the multigram scale.
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Reference:
Benzodioxan,
,1,4-Benzodioxane | C8H8O2 – PubChem