Product Details of 100-19-6. In 2019.0 ADV SYNTH CATAL published article about GRAPHITIC CARBON NITRIDE; PHOTOREDOX CATALYSIS; FABRICATION; REDUCTION; METHANOL; SEMICONDUCTORS; METHYLATION; G-C3N4; BONDS; WATER in [Verma, Fooleswar; Bhardiya, Smita R.; Singh, Manorama; Rai, Vijai K.] Cent Univ, Guru Ghasidas Vishwavidyalaya, Dept Chem, Bilaspur 495009, CG, India; [Shukla, Prashant; Rai, Ankita] Jawaharlal Nehru Univ, Sch Phys Sci, New Delhi 110067, India in 2019.0, Cited 45.0. The Name is 1-(4-Nitrophenyl)ethanone. Through research, I have a further understanding and discovery of 100-19-6.
Unprecedented direct access to terminal enones via alpha-methylenation of aryl ketones to form C=C bond is achieved under visible-light conditions using methanol as one carbon source substrate and solvent as well. The reaction involves Cu@g-C3N4-catalysed in situ oxidation of methanol into formaldehyde followed by dehydrative cross aldol type reaction. Various aryl ketones react efficiently with MeOH, producing alpha,beta-unsaturated carbonyl compounds only in 4-8 h at room temperature in excellent yield (84-97%). Operational simplicity, wide substrate scope, ambient reaction conditions, visible-light photocatalysis and novel application of MeOH as methylene donor substrate are the salient features making the envisaged protocol mild, efficient and green alternative to the existing methods for synthesis of such fine chemicals.
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Reference:
Benzodioxan,
,1,4-Benzodioxane | C8H8O2 – PubChem