Suarez-Pantiga, S; Hernandez-Ruiz, R; Virumbrales, C; Pedrosa, MR; Sanz, R in [Suarez-Pantiga, Samuel; Hernandez-Ruiz, Raquel; Virumbrales, Cintia; Pedrosa, Maria R.; Sanz, Roberto] Univ Burgos, Dept Chem, Pza Misael S-N, Burgos 09001, Spain published Reductive Molybdenum-Catalyzed Direct Amination of Boronic Acids with Nitro Compounds in 2019.0, Cited 64.0. Application In Synthesis of 1-(4-Nitrophenyl)ethanone. The Name is 1-(4-Nitrophenyl)ethanone. Through research, I have a further understanding and discovery of 100-19-6.
The synthesis of aromatic amines is of utmost importance in a wide range of chemical contexts. We report a direct amination of boronic acids with nitro compounds to yield (hetero)aryl amines. The novel combination of a dioxomolybdenum(VI) catalyst and triphenylphosphine as inexpensive reductant has revealed to be decisive to achieve this new C-N coupling. Our methodology has proven to be scalable, air and moisture tolerant, highly chemoselective and engages both aliphatic and aromatic nitro compounds. Moreover, this general and step-economical synthesis of aromatic secondary amines showcases orthogonality to other aromatic amine syntheses as it tolerates aryl halides and carbonyl compounds.
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Reference:
Benzodioxan,
,1,4-Benzodioxane | C8H8O2 – PubChem