Chemo-enzymatic cascade processes are invaluable due to their ability to rapidly construct high-value products from available feedstock chemicals in a one-pot relay manner. In a patent, 274910-19-9, name is (2,3-Dihydrobenzo[b][1,4]dioxin-5-yl)methanol, introducing its new discovery. Recommanded Product: (2,3-Dihydrobenzo[b][1,4]dioxin-5-yl)methanol
Eight new biaryl colchicinoids containing 3?,4?-methylene or benzodioxy ether bridges were synthesized. The key synthetic step employed a ligandless, aqueous Suzuki cross-coupling reaction catalyzed by Pd(OAc) 2 with tetrabutylammonium bromide (TBAB) and potassium carbonate (K2CO3). The biaryl Suzuki products were typically formed in 5-30min and always in less than 1h.
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