Recently I am researching about PORPHYROMONAS-GINGIVALIS ADHERENCE; 1,2,3-TRIAZOLE-BASED INHIBITORS; ORAL STREPTOCOCCI; PROSTAGLANDINS, Saw an article supported by the University of Louisville Dissertation Completion Fellowship; NIH/NIDCRUnited States Department of Health & Human ServicesNational Institutes of Health (NIH) – USANIH National Institute of Dental & Craniofacial Research (NIDCR) [1R01DE023206]; NSFNational Science Foundation (NSF) [CHE1726633]. Published in PERGAMON-ELSEVIER SCIENCE LTD in OXFORD ,Authors: Monsen, PJ; Luzzio, FA. The CAS is 100-19-6. Through research, I have a further understanding and discovery of 1-(4-Nitrophenyl)ethanone. Quality Control of 1-(4-Nitrophenyl)ethanone
An array of arylnitro compounds with various functionality were treated with freshly-prepared aluminum amalgam in THE/water solution and resulted in the corresponding arylamines. The Al(Hg)-mediated reductions are relatively rapid with consumption of the amalgam and disappearance of starting material occurring over 20-30 min. The workup of the reductions involves only removal of the insoluble by-products by filtration followed by concentration. Only in some cases is chromatography required to secure the pure product. The desired arylamines are furnished in quantities of 25-100 mg, which in some cases, could be taken on to the next reaction without further purification. Reductions of 4-nitrobenzyl derivatives of carbohydrates or nucleosides were selective in affording the corresponding 4-aminobenzyl products. To show applicability in click chemistry, selected aminobenzyl products are directly azidated to yield products that were then used in click reactions to afford the corresponding 1,2,3-triazoles. (C) 2020 Elsevier Ltd. All rights reserved.
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Reference:
Benzodioxan,
,1,4-Benzodioxane | C8H8O2 – PubChem