Recently I am researching about C-H-FUNCTIONALIZATION; METAL-FREE; PHOTOREDOX CATALYSIS; OXIDATIVE AMINATION; DIMETHYL-SULFOXIDE; STEREOSELECTIVE-SYNTHESIS; MICHAEL ADDITION; ROOM-TEMPERATURE; FACILE SYNTHESIS; BOND FORMATION, Saw an article supported by the Science and Engineering Research Board (SERB), IndiaDepartment of Science & Technology (India)Science Engineering Research Board (SERB), India [SB/FT/CS073/2014]. Category: benzodioxans. Published in GEORG THIEME VERLAG KG in STUTTGART ,Authors: Rastogi, GK; Deb, ML; Baruah, PK. The CAS is 100-19-6. Through research, I have a further understanding and discovery of 1-(4-Nitrophenyl)ethanone
Here we disclose a simple, visible-light-drivenZ-selective synthesis of methylthio-substituted 1,4-enedione in a single step promoted by Selectfluor. Dimethyl sulfoxide is used as both the ‘thio’ source and the solvent. Molecular iodine and potassium persulfate are used as catalyst and oxidant, respectively. White light (CFL-30W) is used as the light source. The proposed mechanism involves a Kornblum reaction followed by aldol reaction.
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Reference:
Benzodioxan,
,1,4-Benzodioxane | C8H8O2 – PubChem