An article Electrochemical Performance of ABNO for Oxidation of Secondary Alcohols in Acetonitrile Solution WOS:000457150200100 published article about SELECTIVE AEROBIC OXIDATION; ELECTRON-TRANSFER KINETICS; HIGHLY EFFICIENT; BENZYL ALCOHOL; ELECTROCATALYTIC ACTIVITY; TEMPO; ALDEHYDES; CATALYST; ELECTROOXIDATION; NITRILES in [Niu, Pengfei; Liu, Xin; Shen, Zhenlu; Li, Meichao] Zhejiang Univ Technol, Coll Chem Engn, Hangzhou 310032, Zhejiang, Peoples R China; [Niu, Pengfei; Liu, Xin; Li, Meichao] Zhejiang Univ Technol, Res Ctr Anal & Measurement, Hangzhou 310032, Zhejiang, Peoples R China in 2019.0, Cited 72.0. The Name is 1-(4-Nitrophenyl)ethanone. Through research, I have a further understanding and discovery of 100-19-6. Product Details of 100-19-6
The ketones was successfully prepared from secondary alcohols using 9-azabicyclo[3.3.1]nonane-N-oxyl (ABNO) as the catalyst and 2,6-lutidine as the base in acetonitrile solution. The electrochemical activity of ABNO for oxidation of 1-phenylethanol was investigated by cyclic voltammetry, in situ Fourier transform infrared spectroscopy (FTIR) and constant current electrolysis experiments. The resulting cyclic voltammetry indicated that ABNO exhibited much higher electrochemical activity when compared with 2,2,6,6-tetramethylpiperidine-1-oxyl (TEMPO) under the similar conditions. A reasonable reaction mechanism of the electrocatalytic oxidation of 1-phenylethanol to acetophenone was proposed. In addition, a series of secondary alcohols could be converted to the corresponding ketones at room temperature in 80-95% isolated yields.
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Reference:
Benzodioxan,
,1,4-Benzodioxane | C8H8O2 – PubChem