Recommanded Product: 100-19-6. In 2021.0 ADV SYNTH CATAL published article about ASYMMETRIC-SYNTHESIS; DIMETHYL-SULFOXIDE; KETONES in [Li, Hui; Su, Miaodong; Nie, Zhiwen; Yang, Tonglin; Luo, Weiping; Liu, Qiang; Guo, Cancheng] Hunan Univ, Coll Chem & Chem Engn, Changsha 410082, Peoples R China in 2021.0, Cited 41.0. The Name is 1-(4-Nitrophenyl)ethanone. Through research, I have a further understanding and discovery of 100-19-6.
A [3+1+1+1] cycloaddition was developed among 2-arylpropene, ketone and DMSO in the presence of K2S2O8. 2-arylpropene provides three carbons, ketone offers one carbon, and DMSO as dual carbon donor contributes two carbons to the six-membered carbocycle. It gave the cyclohexene motif and spirocyclohexene skeleton. Four C-C bonds formed in this process. Both propylene and ketone could be well tolerated and give the corresponding cyclohexene or spirocyclohexene motif in useful yields. Based on the controlled experiments, a possible mechanism was proposed.
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Reference:
Benzodioxan,
,1,4-Benzodioxane | C8H8O2 – PubChem